By Leonard, John; Lygo, B.; Procter, Garry
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Extra info for Advanced practical organic chemistry
The level of detail needed for compound characterization purposes will depend on the structural complexity of the molecule and on where the data will be reported. For the purpose of a patent application, a molecular mass measurement, evidence of purity, and a good set of NMR data that is in accord with the structure will normally be sufficient. If you aim to publish work in the chemical literature and/or thesis form, you should agree with your supervisor on the standard that is to be adopted. Each journal has its own specific requirements not only for the type of data required but also for the format in which it needs to be presented.
Mol. 3 (uv-active; pet. 1751. 4 A completed data sheet. Chapter three: Keeping records of laboratory work 31 of experimental results. The backbone of any thesis or report in organic chemistry is the body of experimental results that have been gathered during the project. For this reason, the results should be reviewed and evaluated before starting to write the report. 1 Sections of a report or thesis Most detailed organic chemistry reports will consist of three main sections: 1. The Introduction In this section, the project is introduced, the origins of the project and the original objectives are outlined, and all relevant background work is reviewed and referenced.
This may lead to the reaction mixture being expelled from the reaction flask violently. Such problems can normally be avoided by adding a rate-limiting reagent slowly, maintaining the operating temperature of the reaction. 5 Accident and emergency procedures Regrettably, accidents do sometimes happen, so it is vital that you know what to do if an accident does occur. You must be familiar with the firefighting equipment in your laboratory (fire extinguishers, fire blankets, and sand buckets) and you must know the procedures for summoning the fire department and for evacuating the building.
Advanced practical organic chemistry by Leonard, John; Lygo, B.; Procter, Garry